Preparation of tetra- and tri-O-methyl ethers of methyl-α-D-mannopyranoside and their acetates
E. V. Evtushenko, Yu. S. Ovodov
Pacific Institute of Bioorganic Chemistry, Far East Division, Academy of Sciences of the USSR, Vladivostok
Abstract: A convenient technique of preparing tetra- and tri-O-methyl ethers of methyl-α-D-mannopyranoside by its partial methylation followed by liquid chromatography is suggested. All methyl ethers and their acetates were obtained in individual form, 13C NMR spectra are presented.
Russian Journal of Bioorganic Chemistry 1991, 17 (7):973-975