³H NMR analysis of highly tritium-labelled alanine

S. G. Rosenberg, V. M. Zaloznikh, Yu. A. Zolotarev, D. A. Zajtsev, N. F. Myasoedov

Institute of Pharmacology Academy of Medical Sciences of the USSR, Moscow: * Institute of Geochemistry and Analytical Chemistry Academy of Sciences of the USSR, Moscow: ** Institute of Molecular Genetics Academy of Sciences of the USSR, Moscow

Abstract: A method has been developed for the analysis of deuterium oxide solutions of tri-tiated alanine eight-component isotopic mixtures by using high resolution ³H and ¹H NMR spectra at frequences 266,8 and 500,13 MHc, respectively. Approaches have been worked out for the determination of qualitative composition of the mixtures and spectral parameters.

Russian Journal of Bioorganic Chemistry 1990, 16 (6):858-861

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